Fenniri, Hicham, GrigoryA. Tikhomirov, Darren H. Brouwer et al. “High Field Solid-State NMR Spectroscopy Investigation of 15N-Labeled Rosette Nanotubes: Hydrogen Bond Network and Channel-Bound Water.” Journal of the American Chemical Society 138, no. 19 (2016): 6115-6118.
Abstract
15N-labeled rosette nanotubes were synthesized and investigated using high-field solid-state NMR spectroscopy, X-ray diffraction, atomic force microscopy, and electron microscopy. The results established the H-bond network involved in the self-assembly of the nanostructure as well as bound water molecules in the nanotube’s channel.